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Beilstein J. Org. Chem. 2014, 10, 1657–1669, doi:10.3762/bjoc.10.173
Graphical Abstract
Figure 1: The structures of purine nucleosides studied in the chemoenzymatic synthesis and in a cascade one-p...
Scheme 1: Chemical synthesis of 2-deoxy-2-fluoro-α/β-D-arabinofuranose-1-phosphates (12a,b). Reagents and con...
Figure 2: The structures of 1-phosphates of α-D-arabinofuranose (13a; AraFur-1P) and β-D-arabinopyranose (13b...
Figure 3: Geometry optimization of 1-phosphates of 2-deoxy-2-fluoro-α-D-arabinofuranose (12a) and the β-anome...
Figure 4: Progress of the formation of 9-(2-deoxy-2-fluoro-β-D-arabinofuranosyl)-2-chloroadenine (1), 2-amino...
Figure 5: Clofarabine content in the reaction mixture vs time (hours) of the reaction.
Scheme 2: Suggested mechanism of purine nucleoside synthesis catalyzed by E. coli purine nucleoside phosphory...
Figure 6: Progress of the formation of β-D-arabinofuranosides and 2-deoxy-2-fluoro-β-D-arabinofuranosides of ...
Figure 7: Tautomeric structures of 5-aza-7-deazaguanine (17).
Figure 8: Progress of the formation of clofarabine (1), 9-(β-D-arabinofuranosyl)-2-chloroadenine (6), 9-(β-D-...